Positron-emitting isotopes of arsenic, As-70 (T-1/2 = 53 min), As-71 (T-1/2
= 64 h), (72)AS (T-1/2 = 26 h), and As-73 (T-1/2 = 17.8 d) are of interest
in biomedical investigations using PET. A fast and simple method for their
production using low-energy proton and deuteron reactions on enriched Ge-t
argets is presented. Dry distillation of GeO2 at 1105 degreesC during 2 hou
rs provides a separation efficiency of more than 60%. The loss of target ma
terial is less than one per cent and the irradiated targets can be used sev
eral times. The method allows production of diagnostically useful amounts o
f positron-emitting arsenic isotopes using accelerators commonly available
at PET-centres.