Identification and quantitation of anhydrosugars in biomass pyrolytic oilsusing carbon-13 NMR spectroscopy

Authors
Castola, V Bighelli, A Conti, L Scano, G Mascia, S Casanova, J
Citation
V. Castola et al., Identification and quantitation of anhydrosugars in biomass pyrolytic oilsusing carbon-13 NMR spectroscopy, CAN J A S S, 45(4), 2000, pp. 102-107
Citations number
27
Categorie Soggetti
Spectroscopy /Instrumentation/Analytical Sciences
Journal title
CANADIAN JOURNAL OF ANALYTICAL SCIENCES AND SPECTROSCOPY
ISSN journal
12056685 → ACNP
Volume
45
Issue
4
Year of publication
2000
Pages
102 - 107
Database
ISI
SICI code
1205-6685(2000)45:4<102:IAQOAI>2.0.ZU;2-D
Abstract
We described a method which allowed identification and quantitation of anhy drosugars in biomass pyrolysis liquids using carbon-13 NMR spectroscopy. Th e quantitative procedure was checked and validated (accuracy, precision and response linearity) with pure compounds and artificial mixtures. This meth od was then applied to the analysis of the glucidic fraction obtained after a simple and rapid fractionation of the bio oil.