The magnetic spin structure factor of FeF2 has been directly determined fro
m high energy magnetic x-ray diffraction at 115 keV photon energy. A pure s
pin moment of mu = 401(5) mu (B) was observed, which agrees very well with
the spin moment of the free Fe2+ ion and differs significantly from values
of the total magnetic moment obtained by other methods. The magnetic phase
transition of FeF2 has been carefully investigated and values for the criti
cal exponent of the order parameter obtained by other techniques have been
confirmed.