S. Bertrand et al., Influence of strong fiber/coating interfaces on the mechanical behavior and lifetime of Hi-Nicalon/(PyC/SiC)(n)/SiC minicomposites, J AM CERAM, 84(4), 2001, pp. 787-794
Hi-Nicalon fiber-reinforced silicon carbide matrix minicomposites (Hi-Nical
on/SiC) with nanoscale multilayered (PyC/SIG), fiber coatings (also referre
d to as interphases) have been manufactured via pressure pulse chemical vap
or infiltration (P-CVI). Fiber/coating interfaces were strengthened by usin
g treated fibers. The microstructures of the interphases as well as the pro
pagation and deflection of cracks in the interfacial region were investigat
ed by SEM and TEM, Interfacial shear stress was estimated using various met
hods based on either the width of hysteresis loops on unloading-reloading,
crack spacing, or fitting of the force-deformation curve using a micromecha
nics-based model. Tensile behavior at room temperature and lifetime in stat
ic fatigue in air at 700 degreesC were related to the interphase/interface
characteristics.