Oe. Petrov et al., Characterization of calcium phosphate phases obtained during the preparation of sintered biphase Ca-P ceramics, MATER LETT, 48(3-4), 2001, pp. 162-167
A complex of chemical, powder X-ray diffraction (XRD), scanning and transmi
ssion electron microscopic (SEM and TEM) methods is specified for a control
led preparation of calcium-phosphate (Ca-P) biphase ceramics for the needs
of the clinical practice to be used as bone implants. Reproducibility in th
e synthesis of hydroxyapatite + alpha-tertiary calcium phosphate (HAP + alp
ha -TCP) and hydroxyapatite + beta-tertiary calcium phosphate (HAP + P-TCP)
bioceramics is achieved under controlled conditions: the calcium-to-phosph
orus (Ca/P) ratio, the phases contents, and the texture of the sintered mat
erial. (C) 2001 Elsevier Science B.V. All rights reserved.