Deformed V-Ti alloys with 0.3-5 at.%Ti have been characterized by transmiss
ion electron microscopy and X-ray diffraction. A mechanism for Ti segregati
on during annealing, related to the formation of deformation twins, has bee
n identified. Energy-dispersive X-ray spectroscopy indicates strong local c
hanges in Ti content along the twins. Samples post-deformation annealed at
1473 K show Ti segregation and the formation of Ti-rich precipitates which
have been identified using electron microdiffraction and X-ray spectroscopy
. X-ray diffraction measurements reveal changes in the lattice parameter of
the alloys induced by the Ti segregation and the precipitation processes.