Phase shifts in the intensity oscillation of reflection high-energy electro
n diffraction spots provide evidence for monolayer island formation on AlSb
that is caused by sudden changes in surface stoichiometry. High-resolution
scanning tunneling microscopy confirms the interpretation of the phase shi
ft. These results are consistent with a previous structural assignment of t
he AlSb beta (4x3) and alpha (4x3) surface reconstructions and provide guid
elines for producing smooth interfaces in antimonide-based heterostructures
.