Mp. Delamare et al., Natural and artificial low angle grain boundaries with high current-carrying capabilities, IEEE APPL S, 11(1), 2001, pp. 3788-3791
For several years, technical applications of bulk HTS YBCO superconductors
are of growing interest. However, for applications which require a complex
geometry of the monoliths, the Multi-Seeding Melt Growth (MSMG) and the mec
hanical joining of two single-domain tiles becomes necessary. However, thes
e two techniques lead to the formation of a low-angle grain boundary (GB).
The influence of the seed distance (d(S)) on the properties of the GB has b
een studied in order to obtain a precipitate free grain-boundary. On the to
p surface of one monolith, two distances between two seeds were chosen, i.e
. 4mm and 11mm. Regarding d(S)similar to 11mm, some rich-copper phases and
large pores can be observed throughout the Ga In contrast, for d(S)similar
to 4mm, neither residual copper-rich phases nor pores are observed within t
he GB. Magneto-optical measurements performed on the sample with d(S)simila
r to 4mm, revealed that the critical current density through the GB is infl
uenced by the growth directions. Regarding the mechanical joining, a high c
onnectivity between two adjacent domains can be obtained by using the PLD t
echnique for coating of the monoliths.