In this paper we present an experimental method which is well suited to syn
chrotron x-ray diffraction tomography. The experimental technique utilizes
an analyser crystal placed in the diffracted x-ray beam to selectively dete
ct diffracted photons at the desired scattering angle. This arrangement sel
ects the prominent diffraction feature of a specimen component, allowing th
e spatial distribution of that component to be specifically and quantitativ
ely imaged. Images of the spatial variation of the differential x-ray scatt
ering cross section (reflectivity) in a cross sectional plane of interest a
re reconstructed using an iterative algebraic technique and an error functi
onal minimization. Reconstructed images of a well characterized phantom sho
w that material features can be clearly delineated. Images based on the spa
tial variation of x-ray linear attenuation coefficients and differential co
herent scattering cross sections have been reconstructed with approximately
125 mum spatial resolution in the imaging plane.