Laser scattering tomography (LST) is extended to quantitative measurements
and to macroscopic fields. A technique is described to image patterns of su
bmicroscopic scatterers decorating defects in depths up to a few mm without
focus degradation. It is especially useful to reveal the arrangement of pr
ecipitates of low concentration and assures the proportionality between the
measured intensity of the scatterer and its scattering cross-section. The
relative volumes of the submicroscopic precipitates are determined from the
measured intensities. The extended LST technique is demonstrated for GaAs
crystals grown by the vapour pressure controlled Czochralski (VCz) techniqu
e. Statistically relevant histograms of the volumes of submicroscopic As pr
ecipitates are presented. By Fourier analysis planes preferably populated b
q decorated dislocations can be evaluated for their orientation. Dependenci
es along macroscopic dimensions of the samples call be measured, e.g. along
a wafer radius. (C) 2001 Elsevier Science B.V. All rights reserved.