Simple microcalorimeter for measuring microgram samples at low temperatures

Citation
Sg. Doettinger-zech et al., Simple microcalorimeter for measuring microgram samples at low temperatures, REV SCI INS, 72(5), 2001, pp. 2398-2406
Citations number
27
Categorie Soggetti
Spectroscopy /Instrumentation/Analytical Sciences","Instrumentation & Measurement
Journal title
REVIEW OF SCIENTIFIC INSTRUMENTS
ISSN journal
00346748 → ACNP
Volume
72
Issue
5
Year of publication
2001
Pages
2398 - 2406
Database
ISI
SICI code
0034-6748(200105)72:5<2398:SMFMMS>2.0.ZU;2-0
Abstract
An innovative microcalorimeter has been developed for measuring specific he at of very small microgram samples in the temperature range from 1.5 to 50 K and in magnetic fields up to 11 T. The device is built from a commercial sapphire temperature chip (Cernox), which is modified by means of standard microfabrication techniques and which is used as a sample holder, temperatu re sensor, and sample heater. Compared to existing microcalorimeters the si mple design of our instrument allows a fabrication of the device in a few p rocess steps by using facilities present in a standard laboratory clean roo m. As an illustrative example for the performance of our device, the specif ic heat of an underdoped (La1-xSrx)(2)CuO4 and CaRuO3 single crystal has be en measured by means of the relaxation time method as well as the ac method . (C) 2001 American Institute of Physics.