Imaging conditions for reliable measurement of displacement and strain in high-resolution electron microscopy

Citation
Mj. Hytch et T. Plamann, Imaging conditions for reliable measurement of displacement and strain in high-resolution electron microscopy, ULTRAMICROS, 87(4), 2001, pp. 199-212
Citations number
21
Categorie Soggetti
Multidisciplinary,"Spectroscopy /Instrumentation/Analytical Sciences
Journal title
ULTRAMICROSCOPY
ISSN journal
03043991 → ACNP
Volume
87
Issue
4
Year of publication
2001
Pages
199 - 212
Database
ISI
SICI code
0304-3991(200105)87:4<199:ICFRMO>2.0.ZU;2-W
Abstract
We analyse the degree to which the lattice fringe displacements in an image correspond to displacements of the atomic planes in the specimen using len s transfer theory. Our basic assumption is that the exit wave function fait hfully reproduces the displacements of the projected atomic structure. The way this information is imaged by the objective lens is then developed anal ytically. We observe an interchange of amplitude and phase information betw een the original and the reconstructed wave function. For symmetry-related reflections, we show that in the absence of beam amplitude variations, the displacements are imaged perfectly by the objective lens. The theoretical r esults are confirmed using one-dimensional simulations. For the more compli cated case of non-centrosymmetric structures, beam tilts and crystal tilts, we study the implications for slowly varying displacement fields. Errors a re found to be minimised in areas where the contrast of the lattice fringes is highest. Finally, we deduce from these theoretical results a number of practical rules. (C) 2001 Elsevier Science B.V. All rights reserved.