Rapid analysis of cyanuric acid in swim pool waters by high performance liquid chromatography using porous graphitic carbon

Citation
R. Cantu et al., Rapid analysis of cyanuric acid in swim pool waters by high performance liquid chromatography using porous graphitic carbon, CHROMATOGR, 53(7-8), 2001, pp. 454-456
Citations number
13
Categorie Soggetti
Chemistry & Analysis","Spectroscopy /Instrumentation/Analytical Sciences
Journal title
CHROMATOGRAPHIA
ISSN journal
00095893 → ACNP
Volume
53
Issue
7-8
Year of publication
2001
Pages
454 - 456
Database
ISI
SICI code
0009-5893(200104)53:7-8<454:RAOCAI>2.0.ZU;2-U
Abstract
An approach is presented for reducing analysis times of cyanuric acid in sw imming pool waters by high performance liquid chromatography (HPLC). The HP LC method exploits the unique selectivity of porous graphitic carbon (PGC) to fully resolve cyanuric acid from other pool interferences within 10 min. By carefully timing the injections, multiple injections can be made before the end of the initial chromatographic run, more than doubling sample thro ughout. The method utilizes 95% of a 50 mM phosphate buffer solution (pH 9. 1) and 5% methanol (v/v) with UV detection at 213 nm. This approach yielded run times rivaling those of the fastest methods using silica columns, and with the benefits of increased sensitivity.