V. Medina et al., Effect of bonding variables on the shear bond strength and interfacial morphology of a one-bottle adhesive, OPER DENT, 26(3), 2001, pp. 277-286
This study's objectives were: 1) to determine the combination of bonding pr
ocedures (with or without acid etching, moist or dry substrate, one or two
applications of primer/adhesive) that would produce the highest shear bond
strength of Prime & Bond and Dyract AP and 2) to characterize the resin-den
tin/enamel interface produced by these bonding procedures. Ninety-six bovin
e incisors were randomly assigned to eight groups for shear bond testing to
enamel (n=6) and dentin (n=6), Prime & Bond and Dyract AP were applied and
cured following manufacturers' instructions. Shear bond testing was conduc
ted in a Universal Testing Machine. Thirty-two bovine incisors were section
ed to produce blocks with enamel and dentin, then bonded in pairs for evalu
ation of interfacial morphology, They were polished and argon ion-etched us
ing a high-speed argon ion-etching machine and examined by SEM. The groups
where enamel was etched, kept moist or dry and received a single applicatio
n of Prime & Bond produced the highest shear bond strength. Dentin bond str
engths were high in the groups where dentin was etched and kept moist. The
number of Prime & Bond applications had no effect on dentin bond strength.
Acid etching results in better adaptation of Prime & Bond to enamel and den
tin regardless of whether moisture is present.