A new type of functional fibre with high reducing ability toward Au3was prepared by heat treatment of polyacrylonitrile precursor fibre in
inert atmosphere. Both X-ray photoelectron spectroscopy and wide angl
e X-ray diffraction measurements showed that Au3+ was nearly completel
y reduced to Au-0 on the surface of the fibre after impregnation in Au
Cl3 . HCl solution at room temperature. At the same time, the fibre wa
s oxidized. Copyright (C) 1996 Elsevier Science Ltd.