Hypercooling region of the gamma titanium aluminide alloy Ti,,AI,, it as ac
hieved by cyclically superheating the alloy melt in a containerless electro
magnetic levitation apparatus. The maximum undercooling of the alloy melt a
mounted to 345 K;. XRD, TEM, SEM and optical microscopy techniques were ado
pted to investigate the microstructure and identify the phase composition,
The microstructure of the hypercooled alloy was composed of equaxied gamma
phase grains with a mean diameter of 17 nm, The tine microstructure of the
gamma phases produced a large strengthening effect, raising the hardness to
545 on the Vickers scale. The aluminum composition distribution in the hyp
ercooled sample was homogenous except for a small difference between first
solidified regions and boundaries of cracks. X-ray diffraction results show
ed that all peaks of the gamma phase shifted slightly in the direction of s
mall angles, This can be explained by the disordering growth pattern caused
by the rapid solidification process in the hypercooled melt. (C) 2001 Else
vier Science Ltd. Ah rights reserved.