Adherent and insoluble films of oxidized poly(2,5-di-(-2-furyl)-pyrrole) [p
oly(ONO)] have been anodically synthesized on Pt from a 5 mM monomer soluti
on in acetonitrile + water (3:2 v/v) mixture with 0.2 M LiClO4 at 0.016 mA
cm(-2) with a productivity of 1.45 mug mC(-1). Their reduced films have bee
n further obtained in the same electrolyte by applying -0.082 mA cm(-2). Th
e density, conductivity and percentage of doping ClO4- for both oxidized an
d reduced poly(ONO) have been determined.