Bn. Rajnikant,"gupta, Vk",dinesh,"goswami et al., Structural study of 2,4-dichlorobenzanilide - An aromatic substituted amide, I J PA PHYS, 39(5), 2001, pp. 313-315
The crystal structure of the title compound (C13H9NOCl2) has been determine
d by X-ray crystallographic techniques. The compound crystallizes in the tr
iclinic space group P1 with unit cell parameters: a = 9.717(3), b = 10.104(
3), ( = 13.636(3) Angstrom, alpha = 80.36(2), beta = 78.20(2). gamma = 70.0
7(2)degrees, Z = 4. The structure has been solved by direct methods and ref
ined to R = 0.051 for 3310 observed reflections and omegaR(F-2) = 0.149. Th
ere are two crystallographically independent molecules in the asymmetric un
it. In both the molecules, the phenyl rings are planar. The crystal structu
re is stabilized by van der Waals forces.