The sheets or cylinders of Al-V-Fe alloys were prepared by using water-cool
ed copper mould. The mixed structure of nanoscale icosahedral particles emb
edded on the Al matrix was obtained. The precipitation of icosahedral phase
is sensitive to the variation of composition. The volume fraction of icosa
hedral phase increases with increasing the content of V element and Fe elem
ent in the composition range of V2-8% and Fe2-6%, respectively. The cooling
rate affects significantly the formation of icosahedral phase. With increa
sing the thickness from ribbon to 1 mm sheet, the particles size of icosahe
dral phase in Al-V-Fe alloys increases from 20 nm to 50-60 nm. Further incr
easing the thickness of sheets, Al10V intermetallics may precipitate. Both
tensile and compressive yield strength at room temperature were measured. T
he yield strength of Al-V-Fe alloys is up to 800 MPa. The yield strength of
Al-V-Fe alloys improves with increasing the content of V element and Fe el
ement due to the increase of nano-particle of I-phase.