F. Scheppe et al., A new approach to the coloured visualisation of the grain structure of intermetallic NiAl alloys, PRAKT METAL, 37(5), 2000, pp. 271-275
Intermetallic phases on the basis of NiAl demonstrate an excellent chemical
resistance and a good thermodynamic stability in combination with a high m
elting point. As these alloys have in addition comparatively low densities
and also high thermal conductivity, they appear to be promising candidates
for applications in modern ecological and economical energy conversion syst
ems. In the manufacture of polycrystalline components for the high temperat
ure area of stationary gas turbines, the size, above all, of the individual
grains is therefore of great importance.
Various grain refining mechanisms are being investigated in the frame of cu
rrent research projects. To test their effectiveness it was necessary to im
prove the metallography of NiAl alloys in this respect.
In a series of experiments it was shown that using an etchant based on ferr
ous chloride, a differentiation in the colour of the grains in the microstr
ucture of the NiAl alloy was possible with polarised light. Such a microgra
ph can be analysed directly by the interactive image analysis system (IBAS
US 400). This technique results in a very detailed grain size analysis.