A. Delvecchio et al., GLANCING INCIDENCE X-RAY CHARACTERIZATION OF ULTRATHIN YBA2CU3O7-X FILMS FABRICATED BY MODULATED MAGNETRON SPUTTERING, Journal of alloys and compounds, 251(1-2), 1997, pp. 83-86
In high-T-c superconductor ultrathin films and multilayers the superco
nducting current flow is extremely sensitive to the structural quality
of the interfaces and to any surface irregularities. In this work we
present a microstructural and morphological study of ultrathin YBa2Cu3
O7-delta (YBCO) films grown on SrTiO3 substrate. The firms (thickness
<25 nm) are fabricated by magnetron sputtering with a modified process
that arrows a higher grain cohesion and lower surface roughness. The
analyses are performed by using high-angle single crystal diffraction,
low-angle specular reflectivity and atomic force microscopy. The pres
ence of distinct Kiessig fringes in the specular reflectivity spectra
indicates well-defined layer-substrate and layer-air interfaces. Moreo
ver, a surface roughness of about one unit cell is determined. Finally
, no correlation of the substrate and surface interfaces across the la
yer is found.