Pr8Fe88B4 ribbons prepared by melt spinning have been investigated by x-ray
diffraction, differential thermal analysis, thermomagnetic analysis, atom
force microscopy, and superconducting quantum interface device magnetometer
. The results show that the annealed ribbons consist of the Pr2Fe14B and al
pha -Fe phases. The magnetization of soft alpha -Fe phase remains parallel
to the magnetization of the hard Pr2Fe14B phase for fields less than the ex
change field (H-ex). The exchange field in exchange-spring magnets, determi
ned from the demagnetization curves measured at various temperatures, incre
ases with decreasing grain size and measure temperature. The temperature de
pendence of exchange field was analyzed qualitatively by the expression H-e
x = (AK)(1/2)/(M(s)t). (C) 2001 American Institute of Physics.