DSC measurement and HRTEM observation of precipitates in an Al-1.6 mass%Mg2Si alloy

Citation
S. Ikeno et al., DSC measurement and HRTEM observation of precipitates in an Al-1.6 mass%Mg2Si alloy, J JPN METAL, 65(5), 2001, pp. 404-408
Citations number
21
Categorie Soggetti
Metallurgy
Journal title
JOURNAL OF THE JAPAN INSTITUTE OF METALS
ISSN journal
00214876 → ACNP
Volume
65
Issue
5
Year of publication
2001
Pages
404 - 408
Database
ISI
SICI code
0021-4876(200105)65:5<404:DMAHOO>2.0.ZU;2-H
Abstract
Precipitation sequence in an Al-1.6 mass%Mg2Si alloy was investigated by DS C measurement and HRTEM observation, Four exothermic peaks (A, C, D and E) and one endothermic peak (B) were obtained when samples were heated at 10 K /min. Precipitates were confirmed when samples aged to the temperature of e ach peak were observed using HRTEM, and were classified into several types. Products in the region between peaks A and B were classified as GP zones. Precipitates between peaks B and C were classified as the random-type preci pitates. Precipitates at peak C were classified as the parallelogram-type p recipitates. Precipitates at peak D were classified as metastable phase bet a '. Precipitates at peak E were classified as equilibrium phase beta. Alth ough there have been many reports that the beta " phase is formed at peak C , this was not observed in the present study, rather random-type precipitat es were observed. The hardness of samples heated to various temperatures wa s measured. The temperature that resulted in maximum hardness corresponded to the temperature that yielded the maximum amount of random-type precipita tes.