We report the first observation of x-ray powder-diffraction from molec
ular hydrogen in a diamond-anvil cell obtained at the European Synchro
tron Radiation Facility using image-plate recording techniques. The sa
mple was prepared by compression of hydrogen together with nickel powd
er in the high-pressure chamber. This result suggests that structural
phase transitions in solid hydrogen could be studied directly with pow
der x-ray techniques. (C) 1997 American Institute of Physics.