Crystal structure of Schiff base from condensation of 1H-indole-2,3-dione and griest reagent T

Authors
Sun, YQ Yang, RS Zhang, HH Sun, RQ Yang, QY
Citation
Yq. Sun et al., Crystal structure of Schiff base from condensation of 1H-indole-2,3-dione and griest reagent T, CHIN J ST C, 20(4), 2001, pp. 310-312
Citations number
2
Categorie Soggetti
Inorganic & Nuclear Chemistry
Journal title
CHINESE JOURNAL OF STRUCTURAL CHEMISTRY
ISSN journal
02545861 → ACNP
Volume
20
Issue
4
Year of publication
2001
Pages
310 - 312
Database
ISI
SICI code
0254-5861(2001)20:4<310:CSOSBF>2.0.ZU;2-F
Abstract
The crystal and molecular structure of the compound ( C13HgN4O2Cl) from con densation of 1H-indole-2,3-dione and griest reagent T is reported. The titl e compound is monoclinic with space group P2(1) n, 3 a=12.250(2), b=13.631( 2), c=9.777(1)Angstrom, beta =113.506(7)degrees, V=1497.1(4)Angstrom (3), M -r=297.76, D-c=1.321g/cm(3) mu =2.6cm(-1), F(000)=628, Z=4, R=0.0715, wR =0 .1843 (I >2 sigma (l)). The molecule forms a scorpion-like configuration. B ecause of steric hindrance, it is very difficult for some metal ions to for m coordination compounds.