A simple volatization procedure was developed to detect the residual hexane
in solvent extracted soy meals with good precision using the gas chromatog
raphic technique. The study showed that this method released and assayed re
sidual hexane up to one ppm. The deoiled soybean meals from different solve
nt extraction plants were also analyzed for microbial load. These results i
ndicated the presence of Coliforms, Enterobacteriaceae, Staphylococci, Aero
bacter; Bacillus, Aspergillus and Mucor in the isolates.