LINEAR CYCLODEXTRIN-POLY(VINYLAMINE) - SYNTHESIS AND NMR CHARACTERIZATION

Authors
CRINI G TORRI G GUERRINI M MARTEL B LEKCHIRI Y MORCELLET M
Citation
G. Crini et al., LINEAR CYCLODEXTRIN-POLY(VINYLAMINE) - SYNTHESIS AND NMR CHARACTERIZATION, European Polymer Journal, 33(7), 1997, pp. 1143-1151
Citations number
19
Categorie Soggetti
Polymer Sciences
Journal title
European Polymer Journal → ACNP
ISSN journal
00143057
Volume
33
Issue
7
Year of publication
1997
Pages
1143 - 1151
Database
ISI
SICI code
0014-3057(1997)33:7<1143:LC-SAN>2.0.ZU;2-6
Abstract
The synthesis of polymers containing beta-cyclodextrin (beta-CD) resid ues on the side chain is described. Several cyclodextrin-poly(vinylami ne) with various degrees of substitution were synthesized, using the m ono-tosyl derivative of beta-cyclodextrin as reagent. Several factors (reaction time, amounts of the reactants, composition of the solvent) have been studied. A characterization was carried out using D-2 H-1 - H-1 correlation spectroscopy (COSY-TOCSY) and D-2 H-1 - C-13 heteronuc lear correlation (HMQC). (C) 1997 Elsevier Science Ltd.