An aqueous solution of AgNO3 in the presence of ammonia and Fe(CO)(5) is so
nicated under a H-2/Ar mixture, yielding a nanostructured homogeneous phase
of Ag/Fe2O3. This composite material is further reduced at 300 degreesC un
der hydrogen to produce the nanophased Fe/Ag solid mixture. The as-prepared
material, as well as the reduced mixture, is analyzed by various conventio
nal methods. Magnetization loops, ESR. Mossbauer, and magnetoresistance mea
surements are also conducted to determine the magnetic properties of the pr
oducts. (C) 2001 Elsevier Science B.V. All rights reserved.