Y. Okamoto et al., THERMAL-CONDUCTIVITY OF SELF-REINFORCED S ILICON-NITRIDE CONTAINING LARGE GRAINS ALIGNED BY EXTRUSION PRESSING, Nippon Seramikkusu Kyokai gakujutsu ronbunshi, 105(7), 1997, pp. 631-633
beta-Si3N4 containing 0.5 mol%Y2O3 and 0.5 mol%Nd2O3 was seeded with 5
mass% beta-Si3N4 whisker with high aspect ratio and extruded to align
the whiskers. Self-reinforced microstructure composed of well-aligned
large elongated grains in smaller matrix grains was developed by the
grain growth of seeded whiskers during gas-pressure sintering at 2000
degrees C in 30 MPa N-2 for 4h and heat treatment at 2200 degrees C in
30 MPa N-2 for 4h. Room-temperature thermal conductivity was anisotro
pic; 140 W.m(-1).K-1 for parallel to the grain alignment, and 84 W.m(-
1).K-1 for perpendicular to the alignment.