We report on the magnetic susceptibility and electron spin resonance measur
ements on polycrystalline samples of the vanadium oxide VOSb2O4, a quasi-on
e-dimensional S = 1/2 Heisenberg system. The susceptibility vanishes at zer
o temperature, but there is no cusp at the onset of the susceptibility drop
, and the ESR linewidth exhibits an increase characteristic of a phase tran
sition at a much lower temperature. We show that this behaviour is consiste
nt with the formation of a pseudo-gap in a spin-Peierls system in the adiab
atic limit.