We have studied the magnetization changes during the thermal treatment of C
oxCu100-x (x = 10, 15) melt-spun alloys in a Faraday magnetometer. The evol
ution of the magnetization points out that the Co segregation starts at 370
degreesC and finishes at 550 degreesC. Room temperature hysteresis loops a
nd zero field cooling curves performed in a SQUID magnetometer on samples a
s-quenched and annealed at 450 degreesC and 500 degreesC reveal the presenc
e of Co particles, around 2 nm in radius, and a ferromagnetic phase. For sa
mple annealed at 550 degreesC, when the Co segregation has already fmished,
a ferromagnetic behaviour is detected. (C) 2001 Elsevier Science B.V. All
rights reserved.