An investigation of methods for cleaning stainless-steel weights

Citation
Mt. Clarkson et Bj. May, An investigation of methods for cleaning stainless-steel weights, METROLOGIA, 38(2), 2001, pp. 161-171
Citations number
22
Categorie Soggetti
Spectroscopy /Instrumentation/Analytical Sciences","Instrumentation & Measurement
Journal title
METROLOGIA
ISSN journal
00261394 → ACNP
Volume
38
Issue
2
Year of publication
2001
Pages
161 - 171
Database
ISI
SICI code
0026-1394(2001)38:2<161:AIOMFC>2.0.ZU;2-I
Abstract
Four methods for cleaning stainless-steel I kg weights were investigated as part of research aimed at improving the long-term stability of such mass a rtefacts by means of cleaning. Weights were repeatedly cleaned at intervals of 3 to 4 days and changes in mass measured by comparison with other stand ard weights. The most promising method is cleaning in a Soxhlet apparatus u sing ethanol, with a measured standard deviation of 2.5 mug for the change in mass due to cleaning and no resolvable net change in mass after consecut ive cleanings. Similar repeatability was measured for cleaning in an ultras onic bath containing ethanol, and for boiling in water, but average net los ses in mass per cleaning of (1.6 +/- 0.5) mug (1 sigma) and (1.1 +/- 0.6) m ug (1 sigma), respectively, were observed for these methods. Cleaning in a Soxhlet apparatus using water caused mass variations of up to +/- 40 mug. R epeated cleaning produces a recognizable pattern of mass changes that can b e used to confirm successful cleaning of a weight after only two cleanings. Results on the increase in mass following cleaning are also presented.