A method for estimating nanoparticle size by determining the distribution f
unction p(H-n) of hyperfine magnetic fields from data on the Mossbauer spec
trum of Fe-57 nuclei is described. The idea of the method stems from the fa
ct that, owing to the breaking of exchange bonds for surface atoms, their c
ontribution to the total area bounded by the p(H-n) curve can be singled ou
t. The potentialities of the method are illustrated using the data obtained
in experiments with nanoparticles of magnetite. (C) 2001 MAIK "Nauka/ Inte
rperiodica".