Ga. Burley et al., Unequivocal assignment of the fullerene carbons of diethyl 1,2-methano[60]fullerene 61,61-dicarboxylate using 2D INADEQUATE NMR spectroscopy, MAGN RES CH, 39(8), 2001, pp. 466-470
Assignment of all carbons of the [60]fullerene sphere of diethyl 1,2-methna
no[60]fullerene 61,61-dicarboxylate using 2D INADEQUATE NMR spectroscopy is
described. Acquiring the INADEQUATE data with small spectral widths and op
tional F-1 folding with States-TPPI phase implementation provides a conveni
ent route to high-resolution data. A description of the topology of the [60
]fullerene sphere and its comparison with x-ray crystallographic analysis i
s also presented. Copyright (C) 2001 John Wiley & Sons, Ltd.