Pure polymorph C (denoted ITQ-17) resulting from the intergrowth of zeolite
Beta has been synthesized in the presence of Ge from a fluoride-free synth
esis mixture; this shows that fluoride is not necessary to obtain structure
s containing D4MR units that were believed to be stabilised by fluoride; on
the other hand, the presence of Ge directs the synthesis towards the forma
tion of pure polymorph C.