The thermal change of unstable stacking faults (USFs) in ultrafine and high
ly pure beta -SiC powder synthesized by the plasma chemical vapor depositio
n (plasma-CVD) method was studied by high-resolution transmission electron
microscopy (HR-TEM). The number of USFs, which were frequently observed in
as-synthesized powder, decreased at elevated temperatures in an Ar atmosphe
re. In contrast, the number of general stacking faults (GSFs) increased wit
h decreasing number of USFs. Moreover, a type of stacking fault that was ge
ometrically more unstable than USF was observed in the specimen after heat
treatment. In the present study, the annihilation process of USFs observed
in the specimen before heat treatment is discussed.