Study of inhomogeneous radial distribution of defects in As-grown and annealed Czochralski silicon crystals by multi-chroic infrared light scatteringtomography
My. Ma et al., Study of inhomogeneous radial distribution of defects in As-grown and annealed Czochralski silicon crystals by multi-chroic infrared light scatteringtomography, JPN J A P 1, 40(6A), 2001, pp. 4153-4159
Multi-chroic infrared light scattering tomography (MC-IR-LST) and transmiss
ion electron microscopy (TEM) were used to systematically investigate the i
nhomogeneous radial distribution of defects in as-grown and annealed Czochr
alski silicon (CZ-Si) crystals. A new defect morphology of dark stripes obs
erved for the first time by the MC-IR-LST system in a special region in the
as-grown CZ-Si crystal. After annealing the crystal at 1150 degreesC for 1
6 h in an O-2 atmosphere, dark stripes that became scattered in width and d
eep in contrast were clearly visible in an OSF-ring area. The location of t
hese stripes in the as-grown crystal coincided with that in the annealed CZ
-Si crystal, where many stacking faults and oxygen-precipitate-related poly
hedral defects were revealed by TEM analysis. This means that the dark stri
pes were generated during crystal growth as original grown-in defects. Quan
titative measurement of the inhomogeneous radial distribution of defects in
the annealed crystal was made and the characteristics of the defects in di
fferent regions of the crystal were analytically discussed.