The characterisation of thin magnetostrictive multilayers in the nanometers
cale range [(4,5nmTb(40)Fe(60)/9nmFe)x100] demands a surface sensitive anal
ytical technique. A suitable technique is scanning Auger Electron Spectrosc
opy (AES) to determine the elemental composition, the thickness, the presen
ce of interdiffusion between thin layers, or the presence of contamination
at interfaces. Auger sputter depth profiles are obtained by using Xe-Ion bo
mbardment to etch the sample. Sample rotation during sputtering produces sh
allow craters, minimises roughening and enhances depth resolution. In addit
ion, Auger maps of the craters are used to reveal the separated magnetostri
ctive Tb40Fe60 layers and soft magnetic Fe layers.