G. Vonfircks et al., HIGH-RESOLUTION SOLID-STATE F-19 AND N-15 MAS NMR-SPECTRA OF FLUOROAROMATICS AND AROMATIC NITROGEN-HETEROCYCLES PHYSISORBED ON SILICA AND ALUMINA, Journal of organic chemistry, 62(15), 1997, pp. 5074-5079
High-resolution F-19 and N-15 solid State MAS NMR spectra have been ob
tained for fluoro-substituted aromatics and for aromatic nitrogen hete
rocycles, respectively, adsorbed on silica and alumina, where line nar
rowing is due to the high mobility of these systems on the surface of
the porous materials. F-19,F-19 COSY, F-19,C-13 HETCOR, and F-19 --> C
-13 INEPT experiments were successfully performed, and N-15 NMR was me
asured in natural abundance.