Sj. Tu et al., A convenient synthesis of 2-amino-5,6,7,8,-tetrahydro-5-oxo-4-aryl-7,7-dimethyl-4H-benzo-[b]-pyran-3-ethylcarboxylates under microwave irradiation, SYN COMMUN, 31(17), 2001, pp. 2663-2666
A series of 2-amino-5,6,7,8-tetrahydro-5-oxo-4-aryl-7,7-dimethyl-4H-benzo-[
b]-pyran-3-ethylcarboxylates were synthesized by reaction of beta -cyano-be
ta -carbothoxy styrene and 5,5-dimethyl-1,3-cyclo-hexanedione under microwa
ve irradiation without catalyst and solvent.