The limitations of current fabrication methods preclude producing an effici
ent Fresnel phase zone plate optimized for focusing high-energy (> 40 keV)
synchrotron X-ray beams. To get around this difficulty, one can attempt a M
ultiple zone plate setup that distributes the focusing task among more than
one element, each of which can be manufactured. The focusing of 50 keV und
ulator radiation to a 9 x 7 mum(2) spot size with a flux density gain of 24
was achieved using two stacked zone plates precisely aligned with respect
to each other. The instrument was used to record elemental concentration ma
ps of a geological inclusion specimen using X-ray fluorescence. The stacked
zone plate approach is a viable option for microfocusing high-energy X-ray
s. (C) 2001 Elsevier Science B.V. All rights reserved.