Mapping the chemistry in nanostructured materials by energy-filtering transmission electron microscopy (EFTEM)

Citation
F. Hofer et al., Mapping the chemistry in nanostructured materials by energy-filtering transmission electron microscopy (EFTEM), SPECT ACT A, 57(10), 2001, pp. 2061-2069
Citations number
25
Categorie Soggetti
Spectroscopy /Instrumentation/Analytical Sciences
Journal title
SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY
ISSN journal
13861425 → ACNP
Volume
57
Issue
10
Year of publication
2001
Pages
2061 - 2069
Database
ISI
SICI code
1386-1425(20010901)57:10<2061:MTCINM>2.0.ZU;2-W
Abstract
Energy-filtered transmission electron microscopy (EFTEM) can be used to acq uire elemental distribution maps at high lateral resolution within short ac quisition times, which makes it quite efficient for a detailed characteriza tion of nanostructures, as illustrated with examples concerning a nanostruc tured substituted La-based cermet compound and a nanoscale multilayer. In t he first example, we show how phases in a rapidly cooled substituted LaNi5 can be visualized by recording jump ratio images. Secondly, EFTEM was capab le of imaging individual nanoscale layers in a magnetic multilayer consisti ng of 2 nm terbium and 3 nm iron. (C) 2001 Elsevier Science B.V. All rights reserved.