F. Hofer et al., Mapping the chemistry in nanostructured materials by energy-filtering transmission electron microscopy (EFTEM), SPECT ACT A, 57(10), 2001, pp. 2061-2069
Citations number
25
Categorie Soggetti
Spectroscopy /Instrumentation/Analytical Sciences
Journal title
SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY
Energy-filtered transmission electron microscopy (EFTEM) can be used to acq
uire elemental distribution maps at high lateral resolution within short ac
quisition times, which makes it quite efficient for a detailed characteriza
tion of nanostructures, as illustrated with examples concerning a nanostruc
tured substituted La-based cermet compound and a nanoscale multilayer. In t
he first example, we show how phases in a rapidly cooled substituted LaNi5
can be visualized by recording jump ratio images. Secondly, EFTEM was capab
le of imaging individual nanoscale layers in a magnetic multilayer consisti
ng of 2 nm terbium and 3 nm iron. (C) 2001 Elsevier Science B.V. All rights
reserved.