G. Vaccari et al., Cooling crystallization applied to the "extract" of a chromatographic separation process (SMB) of beet raw juice, ZUCKERINDUS, 126(8), 2001, pp. 619-624
The idea that the current technology of beet sugar manufacture needs great
changes in order to make the technology itself more environmentally compati
ble is gaining more and more ground. Such changes concern energy and water
saving, gaseous emissions, and, in particular, the removal of limestone con
sumption and, as a consequence, of waste materials, i.e. carbonation sludge
s. The research of alternative solutions dictates the use of new technologi
es including membrane separation processes, chromatography and cooling crys
tallization. Beet raw juice has been microfiltered without the traditional
calcocarbonic purification step, softened and put through a chromatographic
separation process using a SMB (Simulated Moving Bed) pilot plant. The fra
ction rich in sugar. "extract", has been crystallized through subsequent co
oling crystallization steps with the purpose of obtaining commercial white
sugar. The results of the trials, which emphasize the characteristics of th
e sugar obtained and the crystallization yields, are presented and discusse
d. The morphology of crystals obtained from the different crystallization s
teps is particularly pointed out. In fact, the peculiar composition of the
non-sucrose fraction present in the "extract" promotes the formation of cry
stals showing particular shapes.