A monolithic monochromator-collimator for high-resolution X-ray diffraction

The possibility of finding, for a given X-ray wavelength, the conditions fo r obtaining multiple coplanar reflections in a single block of crystal is i nvestigated. It is found that by introducing a small relative tilt between two parts of the crystal, the conditions for a high-resolution X-ray monoch romator for conventional and synchrotron X-ray sources can be obtained. The design of a new high-resolution monochromator-collimator based on a single crystal, which takes advantage of the existence for almost any wavelength of n and m planes in the single crystal that lie near the Bragg condition, is presented. A weak link between the two reflecting surfaces is used to al ign the crystal planes and to obtain efficient reflections in the dispersiv e configuration. DuMond diagrams are used to evaluate the total diffracted intensity and the resolution of such a monochromator. The experimental resu lts obtained from prototypes made of single crystals of silicon and germani um are in good agreement with theoretical predictions. This new type of mon ochromator offers the advantages of a compact design and simple alignment.