4,5,6,9-tetramethoxy-11-phenyl-10-oxa-11-azatri-cyclo[7.2.2.0(2,7)]trideca-2(7),3,5,12-tetraen-8-one

Authors
Russi, S Mombru, AW Gamenara, D Dias, E Heinzen, H Moyna, P Faccio, R Suescun, L Mariezcurrena, RA
Citation
S. Russi et al., 4,5,6,9-tetramethoxy-11-phenyl-10-oxa-11-azatri-cyclo[7.2.2.0(2,7)]trideca-2(7),3,5,12-tetraen-8-one, ACT CRYST E, 57, 2001, pp. O444-O446
Citations number
11
Categorie Soggetti
Physical Chemistry/Chemical Physics
Journal title
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE
ISSN journal
16005368 → ACNP
Volume
57
Year of publication
2001
Part
5
Pages
O444 - O446
Database
ISI
SICI code
1600-5368(200105)57:<O444:4>2.0.ZU;2-J
Abstract
The crystal structure of the adduct, C21H21NO2, of tetramethylpurpurogallin with nitrosobenzene is reported. The compound exhibits a [3.2.2] bicyclic system corresponding to two seven-membered rings and one six-membered ring in distorted chair, boat and twist-boat conformations, respectively. One in tramolecular and two intermolecular hydrogen bonds direct the packing and s tabilize the molecule.