U. Holzwarth et al., Positron annihilation studies on the migration of deformation induced vacancies in stainless steel AISI 316 L, APPL PHYS A, 73(4), 2001, pp. 467-475
Positron lifetime measurements were carried out at room temperature before
and after isochronous annealing of cylindrical, machined fatigue specimens
and of round slabs of austenitic stainless steel AISI 316 L deformed in com
pression. Annealing experiments are evaluated in terms of vacancy migration
and sinking to grain boundaries and dislocations. The model assumes spheri
cal grains with a homogeneous initial distribution of vacancies. A vacancy
migration enthalpy of H-V(M) = (0.9 +/-0.15) eV was found. It is concluded
that positron trapping at dislocation lines does not significantly contribu
te to positron lifetime measurements at room temperature and that single va
cancies are the dominating positron traps. Positron annihilation depth prof
iling on cross-sectional areas prepared from machined specimens using a pos
itron microprobe with 10 mum spatial resolution shows that machining of cyl
indrical specimens creates vacancies up to 5 mm below the surface.