The determination of several trace elements, including calcium, chromium, c
opper, iron, lead, magnesium, silver, and zinc in an extremely volatile mat
rix was performed by ICP-OES. Tricloro-trifluoroethane was used as the prim
ary solvent due to its similarity to the inhaled anesthetic agents, with hi
gh volatility and low combustibility. The parameters discussed allowed for
a correlation coefficient of each calibration curve for the elements. deter
mined to be within the range of 0.99-1.0. Good recovery of spiked samples w
as obtained, allowing for the determination of elements within a volatile m
atrix.