A superstructure type of crystal for [Zn(C2H8N2)(3)]Cl-2 center dot 2H(2)O

Authors
Wu, DM Lin, X Lu, CZ Zhuang, HH
Citation
Dm. Wu et al., A superstructure type of crystal for [Zn(C2H8N2)(3)]Cl-2 center dot 2H(2)O, CHIN J ST C, 20(5), 2001, pp. 409-412
Citations number
7
Categorie Soggetti
Inorganic & Nuclear Chemistry
Journal title
CHINESE JOURNAL OF STRUCTURAL CHEMISTRY
ISSN journal
02545861 → ACNP
Volume
20
Issue
5
Year of publication
2001
Pages
409 - 412
Database
ISI
SICI code
0254-5861(2001)20:5<409:ASTOCF>2.0.ZU;2-F
Abstract
The colorless crystal of the title compound was obtained in the reaction sy stem containing reagents of Eu2O3, Zn powder, HCl, H2S, Me4NCl, H2O and CH3 COOH. The crystallographic data: M-r=350.60, monoclinic, C2/c, a=26.3749(7) , b=13.9613(5), c=12.9565(4)Angstrom, beta =93.285(1)degrees, V=4763.1 Angs trom (3), Z=12, D-x=1.467g.cm(-3), mu (MoK alpha)=1.885mm(-1), F(000)=2208, R=0.0552. The research result of X-ray single-crystal structure analysis r eveals that the crystal is of a rare superstructure type.