V. Torra et al., Identification of micro-scale calorimetric devices. I. Establishing the experimental rules for accurate measurements, J THERM ANA, 66(1), 2001, pp. 255-264
The miniaturization of the calorimetric devices to 'nano-sized' scale reduc
es progressively the available surface of the heat flux detectors with an i
ncrease in systematic uncertainty. By means of several Joule and laser sign
als, the positional effects in 'liquid microcalorimeter' micro-sized chip a
re evaluated. This allows the introduction of a 3-D coefficient, modifying
the standard Joule sensitivity. The shape factor includes the surface and t
he volume effects.