With a view to eliminating the use of toxic cyanide for electroplating copp
er, a non-cyanide alkaline bath, using triethanolamine as complexant, has b
een investigated. Various steps of bath developments are discussed in this
paper These include stability and immersion deposition characteristics of s
olutions with varying concentrations, Hull cell experiments to arrive at a
plating bath composition and determination of current efficiency and deposi
t nature under varying operating parameters to optimise the deposition cond
itions.